Preprints
https://doi.org/10.5194/egusphere-2022-83
https://doi.org/10.5194/egusphere-2022-83
 
22 Jun 2022
22 Jun 2022
Status: this preprint is open for discussion.

Building a Filter-Wheel Apparatus to Generate Spectroscopic Information from Cathodoluminescence Images Obtained in a Scanning Electron Microscope: Applications in Zircon Geochronology

Kristin Rabosky1, Colin Inglefield1, Elizabeth Balgord2, Sarah Stamps1, Chloe Jones1, Martin Totland1, Brycen Lee1, and Jeremy Mathews1 Kristin Rabosky et al.
  • 1Department of Physics and Astronomy, Weber State University, Ogden, UT, 84408, USA
  • 2Department of Earth and Environmental Sciences, Weber State University, Ogden, UT, 84408, USA

Abstract. We present a simple inexpensive design for a filter wheel to modify a broadband cathodoluminescence (CL) detector in a scanning electron microscope (SEM) to provide spectroscopic information along with image processing and visualization tools that enhances the quality and utility of that imagery. This system was initially tested using a ZnS standard known to produce a strong CL signal in the visible spectrum. Enhanced images and spectroscopic data could also be used for grain and spot targeting of natural zircons that commonly precedes isotopic analysis by laser ablation or ion microprobe. The filter-wheel system was made from inexpensive or 3D printed materials, allows for interchangeable filters for a variety of applications, and the switching between those filters without the user breaking SEM vacuum. The color filtered images were used to create color composite images similar to those generated by higher-end spectrometers with built-in color filtering capability. The embedded data from the RGB pixels of the color filtered images were then used to generate 2D and 3D graphs providing another visual path for comparing relative intensities. A color composite image and associated 3D graphs for a prototypical zircon sample was generated to demonstrate the usefulness of the device and utility of plots. Design documents and specifications for the color filter wheel, and codes to generate images and plots are available on https://weber.edu/cos/instrument_information.html.

Kristin Rabosky et al.

Status: open (until 28 Jul 2022)

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Kristin Rabosky et al.

Kristin Rabosky et al.

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Short summary
This paper outlines the development of a color filter wheel, attached to a broadband CL detector, which allows us to recover spectroscopic information and generate composite color images. The embedded data from the pixels were used to generate 2D and 3D graphs providing multiple visual pathways for comparing relative intensities. The design can be adjusted to accommodate various chamber specifications and expand the capabilities of the broadband CL detectors housed at many institutions.